Analysis of aldosterone by gas-liquid chromatography

Bernard Kliman; Daniel W. Foster

doi:10.1016/0003-2697(62)90068-4

Analysis of aldosterone by gas-liquid chromatography

Bernard Kliman, Daniel W. Foster

Research output: Contribution to journal › Article › peer-review

4 Scopus citations

Abstract

Aldosterone may be analyzed as the 18,21-diacetate derivative in gas chromatography. Results appear to be reproducible on multiple analyses with small quantities of steroid. The product recovered from the column is similar to the 21-monoacetate, but is not identical as shown by paper chromatography and the failure of the compound to be reacetylated to the diacetate.

Original language	English (US)
Pages (from-to)	403-407
Number of pages	5
Journal	Analytical biochemistry
Volume	3
Issue number	5
DOIs	https://doi.org/10.1016/0003-2697(62)90068-4
State	Published - May 1962

ASJC Scopus subject areas

Biophysics
Biochemistry
Molecular Biology
Cell Biology

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10.1016/0003-2697(62)90068-4

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title = "Analysis of aldosterone by gas-liquid chromatography",

abstract = "Aldosterone may be analyzed as the 18,21-diacetate derivative in gas chromatography. Results appear to be reproducible on multiple analyses with small quantities of steroid. The product recovered from the column is similar to the 21-monoacetate, but is not identical as shown by paper chromatography and the failure of the compound to be reacetylated to the diacetate.",

author = "Bernard Kliman and Foster, {Daniel W.}",

note = "Funding Information: Prom the National Heurt Institute und the Nation& Iwtitute of Arthritis und Metabolic Diseases, National Institutes of Health, Public Health Service, United St&es Departmeb of Health, Education rmd We&aye. Bethesda, Maryland",

year = "1962",

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doi = "10.1016/0003-2697(62)90068-4",

language = "English (US)",

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T1 - Analysis of aldosterone by gas-liquid chromatography

AU - Kliman, Bernard

AU - Foster, Daniel W.

N1 - Funding Information: Prom the National Heurt Institute und the Nation& Iwtitute of Arthritis und Metabolic Diseases, National Institutes of Health, Public Health Service, United St&es Departmeb of Health, Education rmd We&aye. Bethesda, Maryland

PY - 1962/5

Y1 - 1962/5

N2 - Aldosterone may be analyzed as the 18,21-diacetate derivative in gas chromatography. Results appear to be reproducible on multiple analyses with small quantities of steroid. The product recovered from the column is similar to the 21-monoacetate, but is not identical as shown by paper chromatography and the failure of the compound to be reacetylated to the diacetate.

AB - Aldosterone may be analyzed as the 18,21-diacetate derivative in gas chromatography. Results appear to be reproducible on multiple analyses with small quantities of steroid. The product recovered from the column is similar to the 21-monoacetate, but is not identical as shown by paper chromatography and the failure of the compound to be reacetylated to the diacetate.

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ER -

Analysis of aldosterone by gas-liquid chromatography

Abstract

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