High-resolution proton solid-state NMR spectroscopy by phase-modulated Lee-Goldburg experiment

Elena Vinogradov; P. K. Madhu; Shimon Vega

doi:10.1016/S0009-2614(99)01174-4

High-resolution proton solid-state NMR spectroscopy by phase-modulated Lee-Goldburg experiment

Elena Vinogradov, P. K. Madhu, Shimon Vega

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374 Scopus citations

Abstract

In this Letter, we present a pulse scheme for coherent averaging of spin-spin interactions called phase-modulated Lee-Goldburg (PMLG) which is aimed at achieving high-resolution proton NMR spectra in the solid state. Our objective is mainly to discuss the design and execution of this experiment and to show some preliminary experimental results as evidence of the far-reaching potentials of this technique.

Original language	English (US)
Pages (from-to)	443-450
Number of pages	8
Journal	Chemical Physics Letters
Volume	314
Issue number	5-6
DOIs	https://doi.org/10.1016/S0009-2614(99)01174-4
State	Published - Dec 10 1999

ASJC Scopus subject areas

General Physics and Astronomy
Physical and Theoretical Chemistry

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10.1016/S0009-2614(99)01174-4

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title = "High-resolution proton solid-state NMR spectroscopy by phase-modulated Lee-Goldburg experiment",

abstract = "In this Letter, we present a pulse scheme for coherent averaging of spin-spin interactions called phase-modulated Lee-Goldburg (PMLG) which is aimed at achieving high-resolution proton NMR spectra in the solid state. Our objective is mainly to discuss the design and execution of this experiment and to show some preliminary experimental results as evidence of the far-reaching potentials of this technique.",

author = "Elena Vinogradov and Madhu, {P. K.} and Shimon Vega",

note = "Funding Information: We would like to thank Prof. L. Frydman for invaluable discussions and Dr. H. F{\"o}erster for advice and help in this work. The Israel Science Foundation is gratefully acknowledged for financial support.",

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T1 - High-resolution proton solid-state NMR spectroscopy by phase-modulated Lee-Goldburg experiment

AU - Vinogradov, Elena

AU - Madhu, P. K.

AU - Vega, Shimon

N1 - Funding Information: We would like to thank Prof. L. Frydman for invaluable discussions and Dr. H. Föerster for advice and help in this work. The Israel Science Foundation is gratefully acknowledged for financial support.

PY - 1999/12/10

Y1 - 1999/12/10

N2 - In this Letter, we present a pulse scheme for coherent averaging of spin-spin interactions called phase-modulated Lee-Goldburg (PMLG) which is aimed at achieving high-resolution proton NMR spectra in the solid state. Our objective is mainly to discuss the design and execution of this experiment and to show some preliminary experimental results as evidence of the far-reaching potentials of this technique.

AB - In this Letter, we present a pulse scheme for coherent averaging of spin-spin interactions called phase-modulated Lee-Goldburg (PMLG) which is aimed at achieving high-resolution proton NMR spectra in the solid state. Our objective is mainly to discuss the design and execution of this experiment and to show some preliminary experimental results as evidence of the far-reaching potentials of this technique.

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JO - Chemical Physics Letters

JF - Chemical Physics Letters

IS - 5-6

ER -

High-resolution proton solid-state NMR spectroscopy by phase-modulated Lee-Goldburg experiment

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