High-resolution proton solid-state NMR spectroscopy by phase-modulated Lee-Goldburg experiment

Elena Vinogradov, P. K. Madhu, Shimon Vega

Research output: Contribution to journalArticle

324 Citations (Scopus)

Abstract

In this Letter, we present a pulse scheme for coherent averaging of spin-spin interactions called phase-modulated Lee-Goldburg (PMLG) which is aimed at achieving high-resolution proton NMR spectra in the solid state. Our objective is mainly to discuss the design and execution of this experiment and to show some preliminary experimental results as evidence of the far-reaching potentials of this technique.

Original languageEnglish (US)
Pages (from-to)443-450
Number of pages8
JournalChemical Physics Letters
Volume314
Issue number5-6
StatePublished - Dec 10 1999

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Nuclear magnetic resonance spectroscopy
Protons
Nuclear magnetic resonance
solid state
nuclear magnetic resonance
protons
high resolution
spectroscopy
Experiments
pulses
interactions

ASJC Scopus subject areas

  • Physical and Theoretical Chemistry
  • Spectroscopy
  • Atomic and Molecular Physics, and Optics

Cite this

High-resolution proton solid-state NMR spectroscopy by phase-modulated Lee-Goldburg experiment. / Vinogradov, Elena; Madhu, P. K.; Vega, Shimon.

In: Chemical Physics Letters, Vol. 314, No. 5-6, 10.12.1999, p. 443-450.

Research output: Contribution to journalArticle

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