Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences

Elena Vinogradov, P. K. Madhu, Shimon Vega

Research output: Contribution to journalArticle

119 Citations (Scopus)

Abstract

We demonstrate here a new windowed multiple pulse sequence for the detection of protons in solid state NMR. Acquisition windows are inserted in the phase modulated Lee-Goldburg scheme (PMLG). This enables one-dimensional acquisition as against two-dimensional in windowless schemes. The pulse scheme, theoretical justifications and experimental spectra of a few samples are presented. In addition two-dimensional proton-proton and carbon-proton correlation experiments are performed with windowed PMLG proton detection.

Original languageEnglish (US)
Pages (from-to)193-202
Number of pages10
JournalChemical Physics Letters
Volume354
Issue number3-4
DOIs
StatePublished - Mar 12 2002

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decoupling
Protons
Nuclear magnetic resonance
Spectroscopy
solid state
nuclear magnetic resonance
protons
spectroscopy
acquisition
pulses
Carbon
carbon
Experiments

ASJC Scopus subject areas

  • Physical and Theoretical Chemistry
  • Spectroscopy
  • Atomic and Molecular Physics, and Optics

Cite this

Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences. / Vinogradov, Elena; Madhu, P. K.; Vega, Shimon.

In: Chemical Physics Letters, Vol. 354, No. 3-4, 12.03.2002, p. 193-202.

Research output: Contribution to journalArticle

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