Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences

Elena Vinogradov, P. K. Madhu, Shimon Vega

Research output: Contribution to journalArticle

120 Scopus citations

Abstract

We demonstrate here a new windowed multiple pulse sequence for the detection of protons in solid state NMR. Acquisition windows are inserted in the phase modulated Lee-Goldburg scheme (PMLG). This enables one-dimensional acquisition as against two-dimensional in windowless schemes. The pulse scheme, theoretical justifications and experimental spectra of a few samples are presented. In addition two-dimensional proton-proton and carbon-proton correlation experiments are performed with windowed PMLG proton detection.

Original languageEnglish (US)
Pages (from-to)193-202
Number of pages10
JournalChemical Physics Letters
Volume354
Issue number3-4
DOIs
StatePublished - Mar 12 2002

ASJC Scopus subject areas

  • Physics and Astronomy(all)
  • Physical and Theoretical Chemistry

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