Preparation of 7-azidocarbonyl-2,4,9-trithiaadamantane by a new thioacetal crown synthetic method

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Abstract

A new method for synthesizing thioacetal crown is reported for the effective synthesis of 7-methoxycarbonyl-2,4,9-trithiaadamantane. Application of this intermediate in the synthesis of 7-azidocarbonyl-2,4,9-trithiaadamantane, a photoreactive surface linker for photolithographic chemical patterning on self-assembled monolayers on gold surfaces, is also reported.

Original languageEnglish (US)
Pages (from-to)105-109
Number of pages5
JournalJournal of Sulfur Chemistry
Volume26
Issue number2
DOIs
StatePublished - Apr 2005

Keywords

  • 2,4,9-trithiaadamamtane
  • 7-azidocarbonyl-2,4,9-trithiaadamantane
  • 7-methoxycarbonyl-2,4,9-trithiaadamantane

ASJC Scopus subject areas

  • Chemistry(all)

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